Evaluation the Effectiveness of CMC and Klucel-E Modified with TiO2 and ZnO Nanoparticles Used for Consolidation the Damaged Paper Maps

Authors

  • Sawsan Sayed Darwish Department of conservation, Faculty of Archaeology, Cairo University, P.O. Box 12613, Giza 12221, Egypt
  • Rushdya Rabee Ali Hassan Department of conservation, Faculty of Archaeology, Cairo University, P.O. Box 12613, Giza 12221, Egypt
  • Abou El Fottouh A. Abdel Hakim Polymer Department, National Research Centre, Dokki, Giza, Egypt
  • Mubarak Charles John Lado Master student, Department of conservation, Faculty of Archaeology, Cairo University, P.O. Box 12613, Giza 12221,Egypt.

Keywords:

cellulose, nanoparticles, FTIR, artificial, mechanical properties

Abstract

The main goal of this work is to study and evaluate the effectiveness of nano titanium dioxide and nano zinc oxide for enhancing the performances of Carboxymethyl cellulose CMC and Klucel-E used as consolidation materials for historical paper maps. Historical map samples dating back to 1817 & 1952 A.D were treated with CMC and Klucel-E loaded with TiO2 nanoparticles and ZnO nanoparticles. Some of the treated samples were submitted to investigation methods and others were submitted to the artificial thermal aging and then to investigation methods to monitor the changes of consolidation materials after accelerated aging test and to evaluate their effect on mechanical, physical and chemical properties of historical  paper samples under effect of  artificial heat  ageing. Visual assessment, pH measurements, Attenuated Total Reflection infrared spectroscopy (FTIR- ATR) study and mechanical properties determination were undertaken, to see if any significant structural or chemical differences could be detected between “untreated”, “treated” and “treated aged” samples. The results showed that no dramatic changes in functional groups on the paper, as monitored by infrared spectroscopy, occurred in the samples before and after treatment; pH values, however, showed that the tested nanocomposites gave good results in decreasing the acidity of the treated paper. The nanocomposites also enhanced optical and mechanical properties of treated samples.

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Published

2020-07-08

How to Cite

Darwish, S. S. ., Ali Hassan, R. R. ., Hakim, A. E. F. A. A. ., & Lado, M. C. J. . (2020). Evaluation the Effectiveness of CMC and Klucel-E Modified with TiO2 and ZnO Nanoparticles Used for Consolidation the Damaged Paper Maps. International Journal of Sciences: Basic and Applied Research (IJSBAR), 52(2), 217–232. Retrieved from https://www.gssrr.org/index.php/JournalOfBasicAndApplied/article/view/11411

Issue

Vol. 52 No. 2 (2020)

Section

Articles

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