D-Optimal Design for Mixture Amount Experiment Involving Split-Plot Design

Authors

  • A. Muthiah Nur Angriany IPB University, Jl. Raya Dramaga, Babakan, Dramaga District, Bogor City, West Java, Indonesia
  • Anik Djuraidah IPB University, Jl. Raya Dramaga, Babakan, Dramaga District, Bogor City, West Java, Indonesia
  • Utami Dyah Syafitri IPB University, Jl. Raya Dramaga, Babakan, Dramaga District, Bogor City, West Java, Indonesia

Keywords:

D-optimal, mixture amount experiment, split-plot design

Abstract

A mixture amount experiment (MAE) is a design that depends on the proportions of the ingredients and the total amounts. The classical MAE contains the classical mixture experiment on each total amount. Consequently, complete randomization is challenging to implement in MAE, so a split-plot design approach was proposed. In the MAE, the whole plot factor is the total amount of mixtures, while the subplot factor is the composition of the ingredients. Another problem in the MAE is if the number of ingredients and total amounts increase, the number of runs increases. The split-plot design with an optimal design approach was proposed. The study aimed to develop a point-exchange algorithm with a split-plot design approach. The case study used is a mixed design consisting of three ingredients and two total amounts of mixtures. The results obtained are that the algorithm compiled in this study produces optimal design points, namely the edge points in the design region.

References

D. C. Montgomery, Design and analysis of experiments. John wiley & sons, 2001.

G. F. Piepel and J. A. Cornell, “Designs for mixture-amount experiments,” J. Qual. Technol., vol. 19, no. 1, pp. 11–28, 1987.

G. F. Piepel, “Models and designs for generalizations of mixture experiments where the response depends on the total amount,” PhD Thesis, University of Florida, 1985.

H. Scheffé, “Experiments with mixtures,” J. R. Stat. Soc. Ser. B Methodol., vol. 20, no. 2, pp. 344–360, 1958.

M. Pal and N. K. Mandal, “Optimum designs for estimation of parameters in a quadratic mixture-amount model,” Commun. Stat.-Theory Methods, vol. 41, no. 4, pp. 665–673, 2012.

B. Jones and P. Goos, “A candidate-set-free algorithm for generating D-optimal split-plot designs,” J. R. Stat. Soc. Ser. C Appl. Stat., vol. 56, no. 3, pp. 347–364, 2007.

S. M. Kowalski, J. A. Cornell, and G. G. Vining, “Split-plot designs and estimation methods for mixture experiments with process variables,” Technometrics, vol. 44, no. 1, pp. 72–79, 2002.

P. Goos, The optimal design of blocked and split-plot experiments, vol. 164. Springer Science & Business Media, 2012.

W. F. Smith, Experimental design for formulation. SIAM, 2005.

F. Triefenbach, “Design of experiments: the D-optimal approach and its implementation as a computer algorithm,” Thesis Bachelor Degree Inf. Commun. Technol. Umea Univ. Swed., 2008.

P. Goos and M. Vanderbroek, “D-optimal split-plot designs with given numbers and sizes of whole plots,” Technometrics, vol. 45, no. 3, pp. 235–245, 2003.

P. Goos and A. N. Donev, “Tailor-made split-plot designs for mixture and process variables,” J. Qual. Technol., vol. 39, no. 4, pp. 326–339, 2007.

G. G. Njoroge, J. A. Simbauni, and J. A. Koske, “An optimal split plot design for performing a mixture process experiment,” Sci. J. Appl. Math. Stat., vol. 5, no. 1, p. 15, 2017.

P. Goos and B. Jones, Optimal design of experiments: a case study approach. John Wiley & Sons, 2011.

A. Atkinson, A. Donev, and R. Tobias, Optimum experimental designs, with SAS, vol. 34. Oxford University Press, 2007.

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Published

2021-12-08

How to Cite

A. Muthiah Nur Angriany, Anik Djuraidah, & Utami Dyah Syafitri. (2021). D-Optimal Design for Mixture Amount Experiment Involving Split-Plot Design. International Journal of Sciences: Basic and Applied Research (IJSBAR), 60(4), 386–397. Retrieved from https://www.gssrr.org/index.php/JournalOfBasicAndApplied/article/view/13561

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